Synthesis and processing
- Glass melting furnaces; Automated robotic glass melting system.
- Pressure chamber/furnaces for thermal treatments (gas flow, vacuum, glove box)
- Powder processing: high-energy planetary ball mills (dry, wet), sieving, mixing, rheometer.
- Heating microscope (shrinkage); Heating stage microscope (in situ crystallization)
- Setups for solution and sol gel synthesis (glove box, rotary evaporator, spin/deep coating)
Thermal analysis
- Rotational viscometry; Dilatometry (horizontal and vertical)
- Thermobalances with simultaneous DSC or DTA; Large thermogravimetric analyser
- Dynamic-mechanic thermal analysis; Rheometer, particle size analysis
Structural and microstructural analysis
- X-ray diffraction, MEV and TEM microscopy (available at Dept. 6 – BAM)
- Laser scanning and light microscopy
- Vertical dilatometry; IR spectrometry (microscopy); Pycnometry (density)
- Mechanical analysis: Resonance frequency damping analysis (RFDA, E, G, µ), double cantilever beam (DCB, crack propagation), Vickers indentation
Spectroscopic characterization
- UV-Vis-NIR spectrometry
- High resolution NMR spectroscopy (available in Dept. 6 - BAM)
- Steady state and time resolved Photoluminescence; quantum yields (in Dept. 1 - BAM)